5AR1
Crystal structure of Cdc11 from Saccharomyces cerevisiae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-01-17 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 187.050, 187.050, 57.960 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.200 - 2.850 |
R-factor | 0.2574 |
Rwork | 0.257 |
R-free | 0.25880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qnr |
RMSD bond length | 0.010 |
RMSD bond angle | 1.200 |
Data reduction software | autoPROC |
Data scaling software | Aimless ((VERSION 0.5.14)) |
Phasing software | MOLREP |
Refinement software | BUSTER (2.10.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 162.000 | 3.000 |
High resolution limit [Å] | 2.850 | 2.850 |
Rmerge | 0.103 | 1.052 |
Number of reflections | 14458 | |
<I/σ(I)> | 21.5 | 1 |
Completeness [%] | 99.9 | 99.2 |
Redundancy | 34.1 | 13.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | PH 5.5 |