5ACI
X-ray Structure of LPMO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-3 |
Synchrotron site | MAX II |
Beamline | I911-3 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 125.460, 125.460, 125.460 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.750 |
R-factor | 0.16634 |
Rwork | 0.165 |
R-free | 0.19545 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4eir |
RMSD bond length | 0.014 |
RMSD bond angle | 1.667 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.800 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.210 | 1.850 |
Number of reflections | 34560 | |
<I/σ(I)> | 21.72 | 2.59 |
Completeness [%] | 99.9 | 100 |
Redundancy | 35.5 | 31.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 3.6M SODIUM CHLORIDE, 100MM CITRIC ACID PH4.0, pH 5.5 |