Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4ZPF

BACE1 in complex with 8-(3-((1-aminopropan-2-yl)oxy)benzyl)-4-(cyclohexylamino)-1-(3-fluorophenyl)-1,3,8-triazaspiro[4.5]dec-3-en-2-one

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 17-ID
Synchrotron siteAPS
Beamline17-ID
Temperature [K]100
Detector technologyCCD
Collection date2005-01-05
DetectorADSC QUANTUM 210
Wavelength(s)1
Spacegroup nameC 2 2 21
Unit cell lengths103.720, 127.403, 77.024
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution26.350 - 1.800
R-factor0.1821
Rwork0.181
R-free0.20120
RMSD bond length0.010
RMSD bond angle1.050
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Refinement softwareBUSTER-TNT (2.11.4)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0001.860
High resolution limit [Å]1.8003.8801.800
Rmerge0.0790.0430.837
Total number of observations454732
Number of reflections47532
<I/σ(I)>15.365.41.7
Completeness [%]99.999.799.9
Redundancy9.6107.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.52931.5M LITHIUM SULFATE, 0.1M HEPES BUFFER,

221051

PDB entries from 2024-06-12

PDB statisticsPDBj update infoContact PDBjnumon