4XX2
Ohr from Xylella fastidiosa in oxidized state
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | LNLS BEAMLINE D03B-MX1 |
| Synchrotron site | LNLS |
| Beamline | D03B-MX1 |
| Temperature [K] | 275 |
| Detector technology | CCD |
| Collection date | 2010-08-10 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1.43 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 87.813, 83.693, 60.766 |
| Unit cell angles | 90.00, 93.67, 90.00 |
Refinement procedure
| Resolution | 60.630 - 2.150 |
| R-factor | 0.17912 |
| Rwork | 0.176 |
| R-free | 0.22642 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1zb8 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.538 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 60.630 | 2.270 |
| High resolution limit [Å] | 2.150 | 2.150 |
| Number of reflections | 23868 | |
| <I/σ(I)> | 13.9 | 3 |
| Completeness [%] | 99.9 | 99.9 |
| Redundancy | 3.1 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | sodium citrate, sodium cacodylate |
