4X09
Structure of human RNase 6 in complex with sulphate anions
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-10-24 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 27.733, 38.860, 97.965 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.122 - 1.722 |
R-factor | 0.1944 |
Rwork | 0.193 |
R-free | 0.22670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2hky |
RMSD bond length | 0.004 |
RMSD bond angle | 0.908 |
Data reduction software | XDS (20140110) |
Data scaling software | Aimless (0.3.11) |
Phasing software | PHENIX (1.9_1692) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.982 | 1.780 |
High resolution limit [Å] | 1.720 | 1.720 |
Rmerge | 0.028 | 0.234 |
Number of reflections | 11717 | |
<I/σ(I)> | 13 | 2.4 |
Completeness [%] | 99.2 | 99 |
Redundancy | 1.96 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 2M AMMONIUM SULPHATE, 0.1M SODIUM, CACODYLATE, 0.05M SODIUM CHLORIDE, PH 6.5, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 293 K |