Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7A |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7A |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Collection date | 1997-07-15 |
Detector | MARRESEARCH |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 69.790, 69.790, 182.340 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 65.180 - 2.400 |
R-factor | 0.21495 |
Rwork | 0.208 |
R-free | 0.27811 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2tct |
RMSD bond length | 0.012 |
RMSD bond angle | 1.535 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.8) |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.800 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.050 | |
Number of reflections | 7162 | |
<I/σ(I)> | 12.7 | 2.3 |
Completeness [%] | 86.0 | 90.8 |
Redundancy | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | PH 8.0 |