4UTK
XenA - reduced - Y183F variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 57.670, 83.450, 157.130 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.835 - 1.440 |
R-factor | 0.1473 |
Rwork | 0.146 |
R-free | 0.17770 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3l5l |
RMSD bond length | 0.011 |
RMSD bond angle | 1.219 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.840 | 1.490 |
High resolution limit [Å] | 1.440 | 1.440 |
Rmerge | 0.060 | 0.580 |
Number of reflections | 68214 | |
<I/σ(I)> | 13.63 | 2.25 |
Completeness [%] | 99.0 | 99.54 |
Redundancy | 3.6 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |