4TKT
Streptomyces platensis isomigrastatin ketosynthase domain MgsF KS6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-03-17 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97913 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 83.331, 83.331, 203.725 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.612 - 2.429 |
R-factor | 0.1854 |
Rwork | 0.183 |
R-free | 0.23780 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.655 |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.470 |
High resolution limit [Å] | 2.429 | 6.590 | 2.429 |
Rmerge | 0.079 | 0.039 | 0.983 |
Total number of observations | 326286 | ||
Number of reflections | 31725 | ||
<I/σ(I)> | 8.2 | ||
Completeness [%] | 99.8 | 97 | 100 |
Redundancy | 10.3 | 9.5 | 10 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 297 | 1.6M Magnesium sulfate, 0.1M MES pH 6.5 |