4RDJ
Crystal structure of Norovirus Boxer P domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-05-28 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0000 |
Spacegroup name | P 61 |
Unit cell lengths | 139.867, 139.867, 64.743 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.377 - 1.500 |
R-factor | 0.1375 |
Rwork | 0.136 |
R-free | 0.16270 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zl7 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.057 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7_650)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.530 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.047 | 0.419 |
Number of reflections | 115571 | |
<I/σ(I)> | 42.9 | 5.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 11.2 | 11 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 290 | 0.1M LiCl, 18% (w/v) PEG 3350, 10% (v/v) MPD, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 290K |