4QQP
Crystal structure of C1QL3 mutant D207A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-06-09 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.008 |
Spacegroup name | H 3 2 |
Unit cell lengths | 76.590, 76.590, 126.210 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.719 - 1.464 |
R-factor | 0.1739 |
Rwork | 0.172 |
R-free | 0.20280 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.144 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 45.720 |
High resolution limit [Å] | 1.460 |
Number of reflections | 22351 |
Completeness [%] | 91.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 292.15 | 30% PEG400, 0.1 Na-acetate, 0.01M CdCl2, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 292.15K |