4PPL
Crystal structure of eCGP123 H193Q variant at pH 7.5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV++ |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 72.560, 83.390, 74.650 |
Unit cell angles | 90.00, 102.19, 90.00 |
Refinement procedure
Resolution | 46.210 - 2.200 |
R-factor | 0.1947 |
Rwork | 0.190 |
R-free | 0.28690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | ECGP123 WITHOUT CHROMOPHORE WATERS AND SUBSTITUTION |
RMSD bond length | 0.010 |
RMSD bond angle | 1.170 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.0) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 46.210 |
High resolution limit [Å] | 2.200 |
Completeness [%] | 99.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.4 | 293 | 21% PEG 3350, 0.2M MgCl2, 0.1M BTP ph 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 293K |