4P4U
Nucleotide-free stalkless-MxA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-08-17 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95 |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 46.330, 77.000, 205.950 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.200 - 1.900 |
R-factor | 0.2126 |
Rwork | 0.210 |
R-free | 0.25909 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.358 |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.200 | 1.930 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 29671 | |
<I/σ(I)> | 24.6 | 1.8 |
Completeness [%] | 99.7 | 95.1 |
Redundancy | 6.9 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9.1 | 291 | 2.0-2.5M Ammonium sulfate, 0.2M AMPSO/KOH pH9.1 |