4OY8
Structure of ScLPMO10B in complex with zinc.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-03-01 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.28 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 67.620, 67.620, 107.290 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.790 - 1.400 |
R-factor | 0.12588 |
Rwork | 0.125 |
R-free | 0.14333 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.400 |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 1.480 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.080 | 0.228 |
Number of reflections | 54273 | |
<I/σ(I)> | 13.6 | 3.6 |
Completeness [%] | 96.0 | 76.7 |
Redundancy | 4.5 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.2 M zinc acetate, 0.1 M sodium cacodylate, 9 % v/v 2-propanol |