Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-05-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97939 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 303.250, 320.730, 667.620 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.999 - 3.502 |
R-factor | 0.2442 |
Rwork | 0.243 |
R-free | 0.29500 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.334 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.21) |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 73.112 |
High resolution limit [Å] | 3.502 |
Number of reflections | 628863 |
<I/σ(I)> | 6 |
Completeness [%] | 99.7 |
Redundancy | 8.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 0.1 M HEPES pH 7.0, 0.1 % Jeffamine ED-2001 and 1.1 M sodium malonate, VAPOR DIFFUSION, HANGING DROP, temperature 298K |