4NWH
Lysozyme UNDER 30 BAR PRESSURE OF XENON
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2011-07-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.980590 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.306, 79.306, 38.072 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.650 |
R-factor | 0.17512 |
Rwork | 0.173 |
R-free | 0.20816 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1c10 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.310 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | REFMAC |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.080 | 1.740 |
High resolution limit [Å] | 1.650 | 1.650 |
Number of reflections | 15059 | |
<I/σ(I)> | 17.7 | 7.3 |
Completeness [%] | 99.6 | 100 |
Redundancy | 6.8 | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH | 4.6 | 300 | 0.1M sodium acetate, 0.6-1.1M NaCl, pH 4.6, BATCH, temperature 300K |