4NWE
Lysozyme UNDER 30 BAR PRESSURE OF NITROUS OXIDE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2009-05-07 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.976 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.188, 79.188, 37.941 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.580 |
R-factor | 0.17102 |
Rwork | 0.170 |
R-free | 0.19994 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1c10 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.325 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | REFMAC |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.640 |
High resolution limit [Å] | 1.580 | 1.580 |
Number of reflections | 17064 | |
<I/σ(I)> | 41.3 | 4.6 |
Completeness [%] | 99.7 | 100 |
Redundancy | 7.3 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH | 4.6 | 300 | 0.1M sodium acetate, 0.6-1.1M NaCl, pH 4.6, BATCH, temperature 300K |