4NL2
Crystal Structure of Listeria monocytogenes Hfq
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2013-05-22 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 63.600, 66.850, 106.510 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.078 - 2.600 |
R-factor | 0.2159 |
Rwork | 0.213 |
R-free | 0.27180 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.481 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.15) |
Phasing software | PHASER (2.5.1) |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 106.510 | 46.078 | 2.740 |
High resolution limit [Å] | 2.600 | 8.220 | 2.600 |
Rmerge | 0.067 | 0.470 | |
Total number of observations | 2690 | 12056 | |
Number of reflections | 14557 | ||
<I/σ(I)> | 10.4 | 6.5 | 1.6 |
Completeness [%] | 100.0 | 99.5 | 100 |
Redundancy | 5.8 | 5.1 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 40% 1,2-propanediol, 100 mM HEPES, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |