4MZM
MazF from S. aureus crystal form I, P212121, 2.1 A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-05-05 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 60.692, 65.190, 112.011 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.480 - 2.100 |
R-factor | 0.177 |
Rwork | 0.175 |
R-free | 0.22800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ne8 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.088 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CCP4 ((PHASER)) |
Refinement software | PHENIX ((phenix.refine: 1.6.1_357)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 56.340 |
High resolution limit [Å] | 2.100 |
Rmerge | 0.104 |
Number of reflections | 26598 |
<I/σ(I)> | 14 |
Completeness [%] | 99.8 |
Redundancy | 5.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.6 | 293 | 0.2 M NH4Ac, 0.1 M NaAc pH 4.6, 30% (w/v) PEG 4000, VAPOR DIFFUSION, HANGING DROP, temperature 293K |