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4MKM

Repeat domains 1 & 2 of Clostridium perfringens Cpe0147

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsAUSTRALIAN SYNCHROTRON BEAMLINE MX1
Synchrotron siteAustralian Synchrotron
BeamlineMX1
Temperature [K]100
Detector technologyCCD
Collection date2012-10-17
DetectorADSC QUANTUM 315r
Wavelength(s)0.95370
Spacegroup nameP 21 21 21
Unit cell lengths48.188, 63.448, 104.984
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution19.620 - 1.750
R-factor0.2009
Rwork0.199
R-free0.22860
Structure solution methodSAD
RMSD bond length0.010
RMSD bond angle1.240
Data reduction softwareXDS
Data scaling softwareSCALA
Phasing softwarePHENIX
Refinement softwareBUSTER (2.10.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]19.6201.840
High resolution limit [Å]1.7501.750
Number of reflections33221
<I/σ(I)>16.9
Completeness [%]99.999.7
Redundancy14.514.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.529112.5% PEG1000, 12.5% PEG 3350, 12.5% MPD, 0.03 M MgCl2, 0.03 M CaCl2- and 0.1 M bicine/Trizma base pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K

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