4KZJ
Crystal Structure of TR3 LBD L449W Mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-04-27 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.402, 76.600, 127.369 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.160 - 2.120 |
R-factor | 0.2142 |
Rwork | 0.212 |
R-free | 0.25040 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.018 |
RMSD bond angle | 1.897 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.160 |
High resolution limit [Å] | 2.120 | 5.750 | 2.120 |
Rmerge | 0.087 | 0.048 | 0.523 |
Number of reflections | 41285 | ||
<I/σ(I)> | 11 | ||
Completeness [%] | 99.0 | 91.8 | 99.9 |
Redundancy | 4.5 | 4.1 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.2 | 277 | PEG 4000, Sodium citrate, Glycerol, pH 4.2, vapor diffusion, temperature 277K |