4KXZ
crystal structure of tgfb2 in complex with GC2008.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-01-25 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.98011 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 131.200, 359.680, 64.630 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.730 - 2.830 |
Rwork | 0.183 |
R-free | 0.22200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.190 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER-TNT |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.730 | 48.730 | 3.000 |
High resolution limit [Å] | 2.830 | 8.370 | 2.830 |
Rmerge | 0.121 | 0.052 | 0.703 |
Number of reflections | 74205 | ||
<I/σ(I)> | 32.17 | 3 | |
Completeness [%] | 99.5 | 99 | 97.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6 | 296 | 35% PEG400, 100mM MES, VAPOR DIFFUSION, temperature 296K, pH 6.0 |