4KT1
Complex of R-spondin 1 with LGR4 extracellular domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2012-07-01 |
Detector | RIGAKU |
Wavelength(s) | 0.97 |
Spacegroup name | P 32 |
Unit cell lengths | 91.376, 91.376, 87.273 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.671 - 2.497 |
R-factor | 0.1626 |
Rwork | 0.160 |
R-free | 0.20860 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3zyo |
RMSD bond length | 0.007 |
RMSD bond angle | 1.159 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.560 |
High resolution limit [Å] | 2.497 | 2.500 |
Number of reflections | 28261 | |
Completeness [%] | 99.9 | 99.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 291 | PEG, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 291K |