4JI7
Crystal Structure of 30S ribosomal subunit from Thermus thermophilus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-02-06 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.98 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 397.808, 397.808, 214.910 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.841 - 3.500 |
R-factor | 0.1604 |
Rwork | 0.158 |
R-free | 0.20110 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.439 |
Data scaling software | XSCALE |
Phasing software | PHENIX (dev_1119) |
Refinement software | PHENIX (dev_1119) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.710 |
High resolution limit [Å] | 3.500 | 10.290 | 3.500 |
Rmerge | 0.120 | 0.049 | 0.988 |
Number of reflections | 214567 | 8878 | 33596 |
<I/σ(I)> | 11.36 | 33.18 | 2.01 |
Completeness [%] | 99.6 | 98.7 | 97.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | MPD , pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |