4HY8
Structures of PR1 and PR2 intermediates from time-resolved laue crystallography
Experimental procedure
Experimental method | LAUE |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID09 |
Synchrotron site | ESRF |
Beamline | ID09 |
Temperature [K] | 288 |
Detector technology | CCD |
Detector | MAR CCD 130 mm |
Wavelength(s) | 0.77-1.24 |
Spacegroup name | P 63 |
Unit cell lengths | 66.833, 66.833, 40.947 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 1.600 |
R-factor | 0.24 |
Rwork | 0.238 |
R-free | 0.27500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.015 |
Data reduction software | LaueView |
Data scaling software | LaueView |
Phasing software | SHELX |
Refinement software | SHELX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.900 | 1.670 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 13809 | |
Completeness [%] | 94.4 | 98.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 2.6M AMMONIUM SULFATE, 50MM SODIUM PHOSPHATE, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |