4GCH
STRUCTURE AND ACTIVITY OF TWO PHOTOREVERSIBLE CINNAMATES BOUND TO CHYMOTRYPSIN
Experimental procedure
Spacegroup name | P 42 21 2 |
Unit cell lengths | 69.700, 69.700, 97.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.000 - 1.900 |
R-factor | 0.209 |
RMSD bond length | 0.021 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.900 * |
Rmerge | 0.052 * |
Number of reflections | 10856 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | other * | 5.6 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | chymotrypsin | 15 (mg/ml) | |
2 | 1 | 1 | sodium cacodylate | 10 (mM) | |
3 | 1 | 1 | cetyltrimethylammonium bromide | 0.75 (%sat) | |
4 | 1 | 1 | ammonium sulfate | 45 (%sat) | |
5 | 1 | 2 | ammonium sulfate | 65 (%sat) |