4G2D
Crystal structure of the hyperthermophilic Sulfolobus islandicus PLL SisLac
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-06-25 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.980 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 47.810, 47.810, 239.100 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.410 - 2.700 |
R-factor | 0.26612 |
Rwork | 0.265 |
R-free | 0.29244 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vc5 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.513 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 41.410 |
High resolution limit [Å] | 2.700 |
Number of reflections | 9436 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 2 M AMMONIUM SULFATE, 0.1 M TRIS, 0.2M LITHIUM SULFATE, PH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 293KK |