4ES4
Crystal structure of YdiV and FlhD complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-06-20 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.97939 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 132.486, 132.486, 145.685 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.165 - 2.900 |
R-factor | 0.2469 |
Rwork | 0.244 |
R-free | 0.28260 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 3TLQ 1g8e |
RMSD bond length | 0.011 |
RMSD bond angle | 1.367 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.6.2_432)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.000 |
High resolution limit [Å] | 2.900 | 6.240 | 2.900 |
Rmerge | 0.050 | 0.748 | |
Number of reflections | 33268 | ||
<I/σ(I)> | 73.13 | 5.03 | |
Completeness [%] | 99.8 | 98.3 | 100 |
Redundancy | 9.9 | 11 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.8 | 293 | 0.1M Na/K phosphate pH5.8, 6% PEG 3000, VAPOR DIFFUSION, HANGING DROP, temperature 293K |