4D80
Metallosphera sedula Vps4 crystal structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-03-29 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 99.700, 127.390, 191.230 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 106.020 - 3.600 |
R-factor | 0.26688 |
Rwork | 0.264 |
R-free | 0.31822 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.716 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | CRANK2 |
Refinement software | REFMAC (5.8.0071) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.000 | 3.800 |
High resolution limit [Å] | 3.600 | 3.600 |
Rmerge | 0.090 | 0.620 |
Number of reflections | 27368 | |
<I/σ(I)> | 8.31 | 1.76 |
Completeness [%] | 99.1 | 99.6 |
Redundancy | 5.3 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 20 MM TRIS, 50 MM NACL, 0.2 M SODIUM MALONATE PH 7, 19% PEG 3350 |