4D3Z
The structure of inactive prolegumain from chinese hamster, trigonal space group.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-06-26 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 50.810, 50.810, 253.590 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.824 - 2.300 |
R-factor | 0.1666 |
Rwork | 0.163 |
R-free | 0.23270 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4fgu |
RMSD bond length | 0.008 |
RMSD bond angle | 1.140 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.360 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.153 | 1.269 |
Number of reflections | 17828 | |
<I/σ(I)> | 15.5 | 2.6 |
Completeness [%] | 99.7 | 100 |
Redundancy | 19.3 | 18.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 0.03 M MGCL2, 0.03 M CACL2, 10%(W/V) PEG 20000, 20%(V/V) PEG 550 MME, 0.1 MOPS/HEPES PH 8.0 |