4CO8
Structure of the DNA binding ETS domain of human ETV4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-01-18 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 50.801, 50.801, 67.660 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.990 - 1.050 |
R-factor | 0.11727 |
Rwork | 0.117 |
R-free | 0.13201 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4bnc |
RMSD bond length | 0.007 |
RMSD bond angle | 1.348 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.800 | 1.070 |
High resolution limit [Å] | 1.050 | 1.050 |
Rmerge | 0.040 | 0.670 |
Number of reflections | 46056 | |
<I/σ(I)> | 21.1 | 2.1 |
Completeness [%] | 96.5 | 67.5 |
Redundancy | 8.8 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.8 M SODIUM CITRATE TRIBASIC, 0.1 M CACODYLATE PH 6.5. |