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4CKM

Structure of the N-terminal domain of Leishmania SAS-6

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyCCD
Collection date2012-04-27
DetectorADSC CCD
Spacegroup nameP 43 21 2
Unit cell lengths84.250, 84.250, 239.940
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution79.490 - 2.150
R-factor0.21024
Rwork0.208
R-free0.24534
Structure solution methodMAD
Starting model (for MR)NONE
RMSD bond length0.010
RMSD bond angle1.349
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareHKL2Map
Refinement softwareREFMAC (5.8.0047)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]48.8602.270
High resolution limit [Å]2.1502.150
Rmerge0.1401.500
Number of reflections48008
<I/σ(I)>7.61.4
Completeness [%]99.9100
Redundancy5.96
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
15.1100 MM BISTRIS PH 5.1, 200 MM MGCL2, 20% (W/V) PEG-3350

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