4C9R
Xenopus ZNRF3 ectodomain in complex with Xenopus RSPO2 Fu1-Fu2 crystal form I
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-02-18 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.990, 81.229, 71.632 |
Unit cell angles | 90.00, 113.00, 90.00 |
Refinement procedure
Resolution | 65.940 - 2.100 |
R-factor | 0.19 |
Rwork | 0.188 |
R-free | 0.24608 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.013 |
RMSD bond angle | 1.604 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 66.000 |
High resolution limit [Å] | 2.100 |
Rmerge | 0.120 |
Number of reflections | 32344 |
<I/σ(I)> | 17.1 |
Completeness [%] | 93.7 |
Redundancy | 17 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |