4BX3
Crystal Structure of murine Chronophin (Pyridoxal Phosphate Phosphatase)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-09-23 |
Detector | MARRESEARCH |
Spacegroup name | I 2 3 |
Unit cell lengths | 167.100, 167.100, 167.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.659 - 2.193 |
R-factor | 0.1725 |
Rwork | 0.171 |
R-free | 0.20670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2oyc |
RMSD bond length | 0.015 |
RMSD bond angle | 1.640 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.660 | 2.310 |
High resolution limit [Å] | 2.190 | 2.190 |
Rmerge | 0.080 | 0.860 |
Number of reflections | 39743 | |
<I/σ(I)> | 12.9 | 2.2 |
Completeness [%] | 99.9 | 99.7 |
Redundancy | 6.8 | 6.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 0.1M IMIDAZOLE PH 8, 0.2M NACL, 1M SODIUM TARTRATE |