4BPH
High resolution crystal structure of Bacillus subtilis DltC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-07-08 |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 49.207, 49.207, 146.264 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.614 - 1.800 |
R-factor | 0.1696 |
Rwork | 0.167 |
R-free | 0.21730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4bpf |
RMSD bond length | 0.004 |
RMSD bond angle | 0.811 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.930 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.090 | 1.280 |
Number of reflections | 10436 | |
<I/σ(I)> | 27.4 | 2.4 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 19.5 | 19.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.6 | 95 MM SODIUM-CITRATE, 19% PEG 4000, 19% 2-PROPANOL, 8% GLYCEROL, PH 5.6 |