4AT6
Fab fragment of antiporphyrin antibody 14H7
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | LURE BEAMLINE DW32 |
Synchrotron site | LURE |
Beamline | DW32 |
Temperature [K] | 277 |
Detector technology | IMAGE PLATE |
Collection date | 1998-05-12 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.203, 228.160, 146.585 |
Unit cell angles | 90.00, 90.11, 90.00 |
Refinement procedure
Resolution | 16.652 - 2.549 |
R-factor | 0.2813 |
Rwork | 0.279 |
R-free | 0.32810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 1MFA AND 1MF |
RMSD bond length | 0.003 |
RMSD bond angle | 0.747 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.640 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.110 | 0.510 |
Number of reflections | 112207 | |
<I/σ(I)> | 7.36 | 2.09 |
Completeness [%] | 93.7 | 87.8 |
Redundancy | 1.19 | 1.17 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 25% PEG 4000, 0.1 M AMMONIUM ACETATE, 0.1 M SODIUM CACODYLATE PH 6.5 |