3ZNH
Crimean Congo Hemorrhagic Fever Virus OTU domain in complex with ubiquitin-propargyl.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-05-10 |
Detector | ADSC CCD |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 146.050, 146.050, 58.530 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 126.480 - 2.300 |
R-factor | 0.21385 |
Rwork | 0.211 |
R-free | 0.27465 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3phw |
RMSD bond length | 0.018 |
RMSD bond angle | 2.029 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.120 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.090 | 0.690 |
Number of reflections | 16479 | |
<I/σ(I)> | 17.6 | 3.6 |
Completeness [%] | 98.6 | 97.4 |
Redundancy | 4.6 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 20-30% PEG 8000, 100 MM NA CACODYLATE PH 6.5, 100 MM MG ACETATE, AND 2% N-OCTYL-BETA-D-GLUCOSIDE. |