3ZHN
Crystal structure of the T6SS lipoprotein TssJ1 from Pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 113 |
Detector technology | IMAGE PLATE |
Collection date | 2011-03-01 |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 38.315, 41.637, 76.947 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 22.750 - 1.400 |
R-factor | 0.1633 |
Rwork | 0.161 |
R-free | 0.20187 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.020 |
RMSD bond angle | 1.978 |
Data reduction software | d*TREK |
Data scaling software | SCALEPACK |
Phasing software | SHELX |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.240 | 1.450 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.096 | 0.460 |
Number of reflections | 24682 | |
<I/σ(I)> | 10.2 | 2.7 |
Completeness [%] | 98.7 | 87 |
Redundancy | 9.27 | 5.61 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.2M FORMATE, 15% PEG 5K MME |