3ZFM
Crystal structure of EphB2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-07-29 |
| Detector | RIGAKU SATURN |
| Spacegroup name | P 1 |
| Unit cell lengths | 34.590, 41.190, 54.470 |
| Unit cell angles | 92.65, 97.15, 114.79 |
Refinement procedure
| Resolution | 21.110 - 2.270 |
| R-factor | 0.2362 |
| Rwork | 0.235 |
| R-free | 0.26340 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.050 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.5) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 37.170 | 2.390 |
| High resolution limit [Å] | 2.270 | 2.270 |
| Rmerge | 0.040 | 0.120 |
| Number of reflections | 45906 | |
| <I/σ(I)> | 25.7 | 10.3 |
| Completeness [%] | 95.1 | 92.6 |
| Redundancy | 3.9 | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
