3SWY
CNGA3 626-672 containing CLZ domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2010-07-28 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 36.750, 37.650, 49.580 |
Unit cell angles | 90.00, 110.88, 90.00 |
Refinement procedure
Resolution | 29.217 - 1.900 |
R-factor | 0.1981 |
Rwork | 0.197 |
R-free | 0.22360 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1zvb |
RMSD bond length | 0.014 |
RMSD bond angle | 1.058 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.15) |
Phasing software | PHASER |
Refinement software | PHENIX (1.7_650) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.324 | 46.324 | 2.000 |
High resolution limit [Å] | 1.900 | 6.010 | 1.900 |
Rmerge | 0.036 | 0.266 | |
Total number of observations | 1086 | 2779 | |
Number of reflections | 10016 | ||
<I/σ(I)> | 9.6 | 12.6 | 2.5 |
Completeness [%] | 98.6 | 97.5 | 92 |
Redundancy | 3.1 | 3.2 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 293 | 20% w/v PEG3350, 200 mM potassium acetate, pH 6.2, VAPOR DIFFUSION, SITTING DROP, temperature 293K |