3ROW
Crystal Structure of Xanthomonas campestri OleA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2010-06-25 |
Detector | MAR scanner 300 mm plate |
Wavelength(s) | 1.03 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 82.204, 85.379, 102.706 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.006 - 1.849 |
R-factor | 0.1613 |
Rwork | 0.160 |
R-free | 0.19120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fk5 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.038 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7_650)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.880 |
High resolution limit [Å] | 1.849 | 1.849 |
Rmerge | 0.055 | 0.385 |
Number of reflections | 61685 | |
<I/σ(I)> | 40.2 | 5.3 |
Completeness [%] | 98.8 | 97.9 |
Redundancy | 8.2 | 8.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.2 | 298 | 18% PEG 8000, 80 mM potassium phosphate dibasic, 100 mM sodium citrate pH 4.2, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |