3POY
Crystal Structure of the alpha-Neurexin-1 ectodomain, LNS 2-6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-15 |
Detector | MARMOSAIC 325 mm CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 199.740, 61.240, 155.580 |
Unit cell angles | 90.00, 121.21, 90.00 |
Refinement procedure
Resolution | 38.560 - 3.020 |
R-factor | 0.21642 |
Rwork | 0.214 |
R-free | 0.26913 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 3BOD 2hob 2r16 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.369 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.564 | 3.130 |
High resolution limit [Å] | 3.020 | 3.020 |
Number of reflections | 31504 | |
<I/σ(I)> | 8.7 | 2 |
Completeness [%] | 97.9 | 99.5 |
Redundancy | 3.4 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 9 | 287 | 12% PEG20000, 100 mM bicine, 1 mM EDTA, 150 mM NaCl , pH 9.0, VAPOR DIFFUSION, temperature 287K |