3PLS
RON in complex with ligand AMP-PNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-11-10 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.0000 |
Spacegroup name | P 41 |
Unit cell lengths | 98.631, 98.631, 45.297 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.320 - 2.240 |
R-factor | 0.2352 |
Rwork | 0.231 |
R-free | 0.28970 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.278 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 98.530 | 2.300 |
High resolution limit [Å] | 2.240 | 2.240 |
Rmerge | 0.052 | 0.509 |
Number of reflections | 21232 | |
Completeness [%] | 89.0 | 54.6 |
Redundancy | 4.6 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 20% PEG2K and 2mM MgCl2, pH 7.5, VAPOR DIFFUSION |