3P1M
Crystal structure of human ferredoxin-1 (FDX1) in complex with iron-sulfur cluster
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-02 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9763 |
Spacegroup name | P 32 |
Unit cell lengths | 76.576, 76.576, 234.410 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.910 - 2.540 |
R-factor | 0.20541 |
Rwork | 0.204 |
R-free | 0.24132 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1cje |
RMSD bond length | 0.014 |
RMSD bond angle | 1.486 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.500 | 2.670 |
High resolution limit [Å] | 2.540 | 2.540 |
Rmerge | 0.111 | 0.721 |
Number of reflections | 50786 | |
<I/σ(I)> | 11.6 | 2 |
Completeness [%] | 99.8 | 99 |
Redundancy | 5.8 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 293.15 | 1.75M Potassium Citrate (K3Cit), pH 7.4, VAPOR DIFFUSION, SITTING DROP, temperature 293.15K |