3OUI
PHD2-R717 with 40787422
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Collection date | 2008-06-15 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.006, 67.795, 79.092 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.700 |
R-factor | 0.19 |
Rwork | 0.188 |
R-free | 0.21700 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.381 |
Refinement software | REFMAC (5.5.0104) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 51.500 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.120 | 0.480 |
Number of reflections | 24090 | |
<I/σ(I)> | 7.7 | |
Completeness [%] | 99.1 | 93.5 |
Redundancy | 5.5 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 2.0 M AMMONIUM SULFATE, 2% PEG 400, 100 MM ACETATE, pH 5.50, VAPOR DIFFUSION, SITTING DROP, temperature 293K |