3OQO
Ccpa-hpr-ser46p-syn cre
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-15 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.150, 105.210, 173.730 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.400 - 2.970 |
R-factor | 0.212 |
Rwork | 0.212 |
R-free | 0.27000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.100 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 105.000 | 3.040 |
High resolution limit [Å] | 2.970 | 2.970 |
Number of reflections | 28585 | |
Completeness [%] | 99.0 | 99 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | PEG 4000, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |