3NVX
Molecular mechanism of guidance cue recognition
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-3 |
Synchrotron site | SSRL |
Beamline | BL9-3 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-03-01 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 51.088, 171.006, 211.175 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.686 - 2.000 |
R-factor | 0.1782 |
Rwork | 0.176 |
R-free | 0.22450 |
Structure solution method | SIRAS |
RMSD bond length | 0.007 |
RMSD bond angle | 1.053 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | PHENIX ((phenix.refine: 1.5_2)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.030 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.053 | 0.156 |
Number of reflections | 62229 | |
<I/σ(I)> | 10.6 | 4.7 |
Completeness [%] | 98.6 | 91.9 |
Redundancy | 3.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 295 | 0.2M Li2SO4, 15% PEG3350, 20% Glycerol, pH 5.0, VAPOR DIFFUSION, SITTING DROP, temperature 295K |