3NMZ
Crystal structure of APC complexed with Asef
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-08 |
Wavelength(s) | 1.000 |
Spacegroup name | H 3 |
Unit cell lengths | 163.175, 163.175, 242.593 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.110 |
High resolution limit [Å] | 3.000 | 6.460 | 3.000 |
Rmerge | 0.057 | 0.041 | 0.406 |
Number of reflections | 46293 | ||
<I/σ(I)> | 15.1 | ||
Completeness [%] | 96.1 | 99.5 | 69.2 |
Redundancy | 5.6 | 5.8 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 277 | 1M lithium sulfate, 0.5M ammonium sulfate, pH 5.6, vapor diffusion, hanging drop, temperature 277K |