Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-03-31 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.978 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 70.785, 95.637, 42.710 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.210 - 1.300 |
R-factor | 0.16982 |
Rwork | 0.169 |
R-free | 0.19144 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2d1e |
RMSD bond length | 0.017 |
RMSD bond angle | 2.043 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.210 | 1.334 |
High resolution limit [Å] | 1.300 | 1.300 |
Number of reflections | 64740 | |
Completeness [%] | 89.8 | 78.68 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 1.7-2.2 M ammonium sulfate, 0.26-0.32 M NaCl, and 0.1 M sodium cacodylate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |