3M7E
Crystal Structure of Plant SLAC1 homolog TehA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-06-01 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | H 3 |
Unit cell lengths | 95.675, 95.675, 136.113 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.000 - 1.800 |
R-factor | 0.158 |
Rwork | 0.157 |
R-free | 0.18300 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.017 |
RMSD bond angle | 1.573 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.073 | 0.731 |
Number of reflections | 42783 | |
<I/σ(I)> | 10.7 | |
Completeness [%] | 99.3 | 94.3 |
Redundancy | 5.1 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 10.2 | 298 | 28% PEG600, 50mM Glycine pH 10.2, VAPOR DIFFUSION, HANGING DROP, temperature 298K |