3M5R
Crystal Structure of Swine Flu Virus NS1 Effector Domain from H1N1 Influenza A/California/07/2009
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-18 |
Detector | NOIR-1 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 73.530, 70.795, 96.685 |
Unit cell angles | 90.00, 110.30, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.000 |
R-factor | 0.208 |
Rwork | 0.207 |
R-free | 0.24400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3f5t |
RMSD bond length | 0.008 |
RMSD bond angle | 1.104 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.6_289) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 100.000 | 100.000 | 2.070 |
High resolution limit [Å] | 2.000 | 4.310 | 2.000 |
Rmerge | 0.061 | 0.036 | 0.496 |
Number of reflections | 61983 | ||
<I/σ(I)> | 18 | ||
Completeness [%] | 100.0 | 99.7 | 100 |
Redundancy | 3.8 | 3.7 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293 | 1.7 M NaCl, 10% Ethanol and 0.1 M hexamine cobalt (III) chloride, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 293K |